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CHINESE CHEMICAL LETTERS

Vol. 15, No. 3, 2004
CONTENTS

Bischler-Napieralski reaction of 2-(3, 4-dimethoxy-2-nitrophenyl)-n-[2-(3, 4-

dimethoxyphenyl) ethyl]-n-[(S)-1-phenylethyl]acetamide accompanied by elimi-

 nation elimination of chiral auxiliary¡­¡­¡­¡­.¡­.H. M. MA, Z. Z. LIU, S. Z. CHEN

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253

Stereoselective synthesis of (Z)-¦Á-bromovinylstannanes and (E)-a- iodovi-

nylstannanes via hydrozirconation of alkynylstannanes¡­.............¡­¡­¡­¡­.¡­.¡­¡­

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­..... M. Z. CAI, H. D. YE, H. ZHAO, C. S. SONG

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257

Synthesis and bioactivity of novel aminomethyl-2- (1, 2, 4-triazol)-4, 4-di-

methyl-3-pentanone (ol) ¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­..¡­¡­¡­¡­¡­......................

¡­¡­¡­¡­¡­........¡­¡­.¡­S. W. WANG, B. J. SHI, Y. C. LI, Q. M. WANG, R. Q. HUANG

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261

Toward total synthesis of yohimbine and reserpine alkaloids; part 1. An improved synthesis of cis-5, 8-dihydroxy-1, 4, 5, 8, 9,10 hexahydro-naph-thalene-1, 

8-lactone via selective reduction  of the conjugated  ketone with Zn (BH4) 2  ¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.......¡­.¡­............................¡­...Y. Y. LI, M. XU, F. E. CHEN

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265

Synthesis of 7a-aza-benzo[fg]naphthacen-7-one¡­¡­¡­¡­..¡­¡­¡­¡­¡­..¡­¡­

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­......C. G. ZHANG, B. G. LI, X. G. ZHOU, G. L. ZHANG

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269

Synthesize of 2, 6-di-O-acetyl sucrose by regioselective acetylation with di-butyltin oxide¡­¡­¡­¡­..¡­¡­¡­¡­¡­¡­¡­¡­..........¡­¡­...Y. KE, H. M. LIU, Z. Z. LIU

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273

Solid-phase synthesis of acrylamide using polymer- supported ¦Â-selenopro-

pionic acid¡­¡­..............................¡­S. R. SHENG, X. C. WANG, X. L. LIU, X. HUANG

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275

Yb(OTf)3 catalyzed nucleophilic conjugate addition of pyrrole to a, b-un-

saturated ketones and nitro-compounds¡­¡­¡­.............¡­.¡­....P. P. SUN, Y. P. XIAO

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277

A rapid parallel synthesis of 2-dialkylamino-4(3H)-quinazolinones¡­¡­¡­...

¡­...¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­....M. W. DING, Y. LIU, G. F. ZHANG, S. J. YANG

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280

Facile synthesis of 1, 2-diazepine derivatives under microwaveirradiation¡­

¡­¡­¡­¡­¡­..........¡­¡­¡­¡­¡­¡­....¡­J. X. WANG, X. N. SHI, K. H. WANG, X. Q. MEN

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284

Microwave-promoted palladium catalyzed Suzuki cross-coupling reaction in water   ¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­................................¡­¡­.¡­..L. BAI, J. X. WANG

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286

Synthesis of 1-bromo-3-methoxy-4-propoxy-5-iodobenzene¡ªa novel effici-

ent process for the synthesis of brominated aromatic compound¡­.¡­¡­¡­..

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­..............¡­¡­H. X. SHI, H. LIN, G. MANDVILLE

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288

 Synthesis, structures and coordination behavior of central hydroxyl group containing polydentate ligands¡­¡­¡­¡­¡­.................¡­¡­..¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.......¡­J. JIA, X. W. WANG, Y. L. ZHAO, Y. ZHU, J. C. TAO

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292

Oxidation of styrene with molecular oxygen in supercritical CO2¡­..¡­............¡­...

¡­......T. JIANG, B. X. HAN, G. Y. ZHAO, Z. H. LI, Y. H. CHANG, H. X. GAO, J. C. LI

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296

Synthesis of nucleoside derivatives containing benzophenoxazinone moiety

¡­¡­¡­¡­.¡­¡­...¡­¡­¡­Y. GAO, W. X. ZOU, L. WU, J. S. LI, J. T. WANG, J. B. MENG

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300

Huperzine V, a new lycopodium alkaloid from Huperzia serrata ¡­¡­¡­¡­...........¡­

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­...¡­H. Q. LIU, C. H. TAN, S. H. JIANG, D. Y. ZHU

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303

Terresoxazine, a novel compound with benzoxazine skeleton from Tribulus terrestris¡­¡­¡­¡­¡­¡­........¡­.¡­..J. W. HUANG, C. H. TAN, S. H. JIANG, D. Y. ZHU

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305

A new taxoid from leaves and branches of Taxus chinensis¡­¡­¡­¡­...........¡­¡­¡­¡­

¡­¡­¡­¡­¡­......¡­.F. S. WANG, L. Y. PENG, Y. ZHAO, Q. S. ZHAO, K. GU, H. D. SUN

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307

Intercedenol A and B, two new triterpenoids from the sea cucumber Men-samaria intercedens¡­¡­¡­...................................¡­¡­¡­¡­¡­¡­¡­¡­¡­..¡­¡­.¡­¡­¡­¡­¡­¡­..¡­..

¡­¡­¡­¡­.......¡­.Z. R. ZOU, Y. H. YI, H. M. WU, J. H. WU, D. Z. ZHOU, S. Y. ZHANG

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309

Two new phloroglucinol glycosides from Lysidice rhodostega hance¡­.........¡­.¡­..

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.......¡­..S. GAO, S. S. YU, D. Q. YU

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313

A new sesquiterpene-substituted benzoic acid from the brown alga Dicty-opteris divaricata...................F.H. SONG, X. FAN, X. L. XU, J. L. ZHAO, L. J. HAN, J. G. SHI

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316

Selective determination of nanogram g¨Cglobulin in human blood serum by resonance light scattering of  functionalized nano¨CPbS¡­¡­............¡­¡­¡­¡­¡­¡­¡­

¡­¡­¡­¡­¡­¡­¡­...¡­L. Y. WANG, H. Q. CHEN, L. LI, L. DONG, T. T. XIA, L. WANG 

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319

Multianalyte biosensors for the simultaneous determination of glucose and galactose based on thin film electrodes¡­¡­¡­¡­...............¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.¡­.

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.¡­..¡­.N. Q. JIA, Z. R. ZHANG, J. Z. ZHU, G. X. ZHANG

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322

The chemical speciation and behavior of mercury and selenium in the in-

soluble fraction of striped dolphin liver¡­¡­.............¡­X. R. HU, H. LI, Y. X. ZHANG

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326

Preparation of  PVA/ H3PW12O40 fiber mats¡­¡­¡­¡­¡­............¡­.¡­¡­¡­¡­¡­¡­¡­

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­....¡­..¡­J. GONG, C. L. SHAO, G. C. YANG, Y. PAN, L. Y. QU

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330

Synthesis and characterization of organophosphazene polyoxotungstate [(N3P3)(SIW11O39H2)3]12-¡­¡­¡­¡­¡­¡­...................¡­¡­¡­. J. GONG, C. L. SHAO, L. Y. QU

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333

A novel white light emitting long-lasting phosphor¡­¡­¡­..............¡­..¡­¡­¡­¡­¡­¡­.

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­......¡­¡­..¡­¡­.B. F. LEI, Y. L. LIU, Z. R. YE, C. S. SHI

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335

Room temperature phosphorescence of 1-bromo-4-(bromoacetyl) naph-

thalene induced by sodium deoxycholate¡­¡­¡­¡­¡­................¡­¡­¡­¡­¡­¡­...¡­¡­¡­

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­....¡­¡­¡­Y. WANG, W. J. JIN, J. B. CHAO, L. P. QIN

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339

Direct observation of non-covalent complexes for phosphorylated flavor

noidprotein interaction by ESI¡­¡­¡­¡­¡­¡­¡­..¡­¡­¡­¡­¡­¡­..................¡­¡­¡­¡­¡­.

¡­¡­¡­¡­¡­¡­...¡­X. L. CHEN, T. ZHANG, H. X. LIU, L. B. QU, Y. Z. YU,Y. F. ZHAO

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343

A modified chitosan adsorbent for selective removal of low density lipopro-tein¡­..........................................................................................................................

................G. Q. FU, K. Y. SHI, Z. YUAN, W. Q. NIU, B. L. HE, B. LIU, B. SHEN, Y. LIU

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347

A new reaction-controlled phase-transfer catalyst system¡­¡­¡­.............¡­¡­¡­¡­...

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­....¡­..M. Q. LI, X. G. JIAN, G. M. WANG, Y. YU

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350

Reaction of 1, 1-di-p-methoxyphenyl-2, 2-dinitroethylene and 1, 1-di-O-me-

thoxyphenyl-2, 2-dinitroethylene with 1-benzyl-1, 4-dihydronicotinamide: evidence for concerted electron-hydrogen atom transfer mechanism¡­..............................¡­¡­

¡­¡­¡­¡­¡­¡­....¡­D. M. DAI, Y. C. LIU, J. LI, P. WANG, X. D. CHEN,  T. C. W. MAK

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353

Synthesis of metal porphyrins tailed with salicylic acid and their interac-tion with bovine serum albumin ¡­.........................¡­¡­T. JIA, K. WANG, Y. M. ZHAO, Z. Y. LI

 

357

Studies on phase behavior of alkyl polyglucoside based on microemulsions with modified fishlike phase diagram¡­¡­¡­¡­¡­.......................¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­.

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­....¡­..J. L. CHAI, G. Z. LI, Z. Y. DIAO, G. Y. ZHANG

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361

A novel method for making NiO nanofibres via an electrospinning technique

¡­¡­...........¡­.C. L. SHAO, H. Y. GUAN, S. B. WEN, B. CHEN, X. H. YANG, J. GONG

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365

Photocatalytic hydrogen and oxygen formation from water over Ga-modi-fied zeolite ¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­......................¡­¡­¡­..C. H. HE, O. B. YANG

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368

 A novel method for preparing approximately micron-sized polymethyl methacrylate microspheres with clear surface¡­¡­¡­¡­..............¡­¡­..¡­¡­¡­¡­¡­¡­

¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­¡­...¡­...D. Q. WANG, B. L. LIU, J. HU, X. Q. LIN, M. ZHANG

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371

Synthesis of new naphthaline-type chromophores with strong green-emit-ting or the blue-emitting in b-cyclodextrin¡­¡­¡­¡­¡­............................¡­..¡­¡­.¡­¡­¡­...¡­.

¡­¡­....¡­.Q. F. SHI, X. M. WANG, K. J. PAN, W. L. JIANG, D. J. WEN,  X. B. WANG

 

 

375